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Each batch includes a COA with HPLC chromatogram and MS molecular weight confirmation

The gradient was programmed to: 01.0 min 99% A, 110 min to 1% A, 1011.5 min hold 1% A, 11.513.5 min hold 99% A

Reference: Chang CH, Tsai WC, Lin MS, Hsu YH, Pang JHS